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How to figure out why BTRFS drive reports it is out of space
(lemmy.sdf.org)
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Looking at balancing might be right place to start. ref, https://archive.kernel.org/oldwiki/btrfs.wiki.kernel.org/index.php/FAQ.html#Help.21_I_ran_out_of_disk_space.21
You might want to start by rebalancing by percentages and not all at once. If nothing else it'll tell you much sooner if you're on the right track or not. Something like
sudo btrfs balance start -dusage=20 -musage=20 /mnt/disk3
to work on only blocks that are 20% full or less. That should coaleace them into single data blocks and free up some others.